6I06
Crystal structure of psychrophilic phosphoglycerate kinase from Pseudomonas TACII18
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM30A |
Synchrotron site | ESRF |
Beamline | BM30A |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2000-03-31 |
Detector | MARRESEARCH |
Wavelength(s) | 0.90005 |
Spacegroup name | P 32 |
格子定数 [Å] | 59.100, 59.100, 87.000 |
格子定数 [度] | 90.00, 90.00, 120.00 |
精密化法
残基 | 29.550 - 2.000 |
R因子 | 0.1815 |
Rwork | 0.179 |
R-free | 0.22890 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 6hxe |
結合長の平均二乗偏差(RMSD) [Å] | 0.002 |
結合角の平均二乗偏差(RMSD) [度] | 0.479 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | PHENIX ((1.14_3260: ???)) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 29.550 | 2.090 |
分解能 [Å] (高) | 2.000 | 2.000 |
Rmerge_l_obs | 0.095 | |
独立反射数 | 23306 | |
<I/σ(I)> | 12 | |
完全性 [%] | 99.9 | |
冗長性 | 2.8 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 290 | 20% PEG 10000 and 0.1 M HEPES at pH 7.5 |