6GG7
cyanobacterial GAPDH with full-length CP12
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-02-27 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.96861 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 141.052, 141.052, 75.931 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 60.416 - 1.320 |
R-factor | 0.1468 |
Rwork | 0.145 |
R-free | 0.17350 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4boy |
RMSD bond length | 0.005 |
RMSD bond angle | 0.921 |
Data reduction software | xia2 |
Data scaling software | xia2 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.13_2998: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 60.420 | 1.367 |
High resolution limit [Å] | 1.320 | 1.320 |
Rmerge | 0.127 | 0.918 |
Rmeas | 0.132 | 0.957 |
Number of reflections | 178371 | 17624 |
<I/σ(I)> | 11.43 | |
Completeness [%] | 100.0 | 100 |
Redundancy | 12.8 | 12.6 |
CC(1/2) | 0.988 | 0.586 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 290 | Tryptone CM1(A6) 1% Tryptone, 25% PEG, 100 mM Hepes pH 8. |