6FPT
Crystal structure of Danio rerio Lin41 filamin-NHL domains
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-07-15 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 1.260 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 65.800, 90.590, 131.050 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.430 - 2.600 |
R-factor | 0.1847 |
Rwork | 0.181 |
R-free | 0.24390 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | Homology models based on PDB IDs 4UMG and 1Q7F |
RMSD bond length | 0.010 |
RMSD bond angle | 1.200 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | BUSTER (2.11.5) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.670 |
High resolution limit [Å] | 2.600 | 2.600 |
Number of reflections | 42647 | 3006 |
<I/σ(I)> | 5.28 | |
Completeness [%] | 91.6 | 86.8 |
Redundancy | 1.9 | 1.8 |
CC(1/2) | 0.987 | 0.779 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 293 | 10% PEG 8000 0.2 M magnesium chloride 0.1 M Tris pH 7.0 0.1 M trisodium citrate |