6FPT
Crystal structure of Danio rerio Lin41 filamin-NHL domains
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-07-15 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 1.260 |
Spacegroup name | P 21 21 21 |
格子定数 [Å] | 65.800, 90.590, 131.050 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 46.430 - 2.600 |
R因子 | 0.1847 |
Rwork | 0.181 |
R-free | 0.24390 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | Homology models based on PDB IDs 4UMG and 1Q7F |
結合長の平均二乗偏差(RMSD) [Å] | 0.010 |
結合角の平均二乗偏差(RMSD) [度] | 1.200 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | BUSTER (2.11.5) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 50.000 | 2.670 |
分解能 [Å] (高) | 2.600 | 2.600 |
独立反射数 | 42647 | 3006 |
<I/σ(I)> | 5.28 | |
完全性 [%] | 91.6 | 86.8 |
冗長性 | 1.9 | 1.8 |
CC(1/2) | 0.987 | 0.779 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 293 | 10% PEG 8000 0.2 M magnesium chloride 0.1 M Tris pH 7.0 0.1 M trisodium citrate |