6FMT
IMISX-EP of Hg-BacA Soaking SAD
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-12-15 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.9 |
Spacegroup name | C 2 2 2 |
格子定数 [Å] | 112.620, 145.550, 40.330 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 44.558 - 3.000 |
R因子 | 0.2378 |
Rwork | 0.236 |
R-free | 0.27760 |
Structure solution method | SAD |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | SHELXCD |
Refinement software | PHENIX ((1.13rc1_2954: ???)) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 44.580 | 3.080 |
分解能 [Å] (高) | 3.000 | 3.000 |
Rmeas | 0.480 | 3.930 |
独立反射数 | 12841 | 977 |
<I/σ(I)> | 10.62 | 1.97 |
完全性 [%] | 100.0 | 100 |
冗長性 | 65.4 | 60.7 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | LIPIDIC CUBIC PHASE | 293 | 40 % PEG-400, 0.3-0.5 M ammonium citrate dibasic and 0.1 M sodium citrate pH 5.0 |