6DHE
RT XFEL structure of the dark-stable state of Photosystem II (0F, S1-rich) at 2.05 Angstrom resolution
これはPDB形式変換不可エントリーです。
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | FREE ELECTRON LASER |
Source details | SLAC LCLS BEAMLINE MFX |
Synchrotron site | SLAC LCLS |
Beamline | MFX |
Temperature [K] | 298 |
Detector technology | CCD |
Collection date | 2016-07-14 |
Detector | RAYONIX MX170-HS |
Wavelength(s) | 1.305 |
Spacegroup name | P 21 21 21 |
格子定数 [Å] | 116.906, 221.407, 308.668 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 30.552 - 2.050 |
R因子 | 0.1851 |
Rwork | 0.185 |
R-free | 0.24130 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5kaf |
Data reduction software | cctbx.xfel |
Phasing software | PHASER (dev_svn) |
Refinement software | PHENIX (dev_svn) |
Quality characteristics
Overall | Inner shell | Outer shell | |
分解能 [Å] (低) | 30.550 | 30.550 | 2.085 |
分解能 [Å] (高) | 2.050 | 5.565 | 2.050 |
独立反射数 | 497372 | ||
<I/σ(I)> | 16.581 | 132.601 | 0.53 |
完全性 [%] | 100.0 | 99.24 | 99.95 |
冗長性 | 245.79 | 896.6 | 12.58 |
CC(1/2) | 0.987 | 0.993 | 0.018 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | BATCH MODE | 6.5 | 298 | 0.1 M MES pH 6.5, 0.1 M NH4Cl, 35% (w/v) PEG 5000 |
1 | BATCH MODE | 6.5 | 298 | 0.1 M MES pH 6.5, 0.1 M NH4Cl, 35% (w/v) PEG 5000 |
1 | BATCH MODE | 6.5 | 298 | 0.1 M MES pH 6.5, 0.1 M NH4Cl, 35% (w/v) PEG 5000 |