6AVS
Complex structure of JMJD5 and Symmetric Monomethyl-Arginine (MMA)
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2017-03-23 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9795 |
Spacegroup name | P 21 21 21 |
格子定数 [Å] | 49.685, 65.063, 78.139 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 50.000 - 2.020 |
R因子 | 0.244 |
Rwork | 0.241 |
R-free | 0.27200 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5fbj |
結合長の平均二乗偏差(RMSD) [Å] | 0.026 |
結合角の平均二乗偏差(RMSD) [度] | 1.917 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Quality characteristics
Overall | |
分解能 [Å] (低) | 49.999 |
分解能 [Å] (高) | 2.000 |
独立反射数 | 17227 |
<I/σ(I)> | 10.64 |
完全性 [%] | 99.0 |
冗長性 | 6.5 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | 0.1M HEPES pH 7.0 8% PEG 3350 |