5Z5K
Structure of the DCC-Draxin complex
Experimental procedure
| 実験手法 | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL17U1 |
| Synchrotron site | SSRF |
| Beamline | BL17U1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2015-08-15 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 1 |
| Spacegroup name | P 65 |
| 格子定数 [Å] | 108.069, 108.069, 130.266 |
| 格子定数 [度] | 90.00, 90.00, 120.00 |
精密化法
| 残基 | 35.374 - 2.493 |
| R因子 | 0.2143 |
| Rwork | 0.212 |
| R-free | 0.24750 |
| Structure solution method | MOLECULAR REPLACEMENT |
| 結合長の平均二乗偏差(RMSD) [Å] | 0.003 |
| 結合角の平均二乗偏差(RMSD) [度] | 0.581 |
| Data scaling software | SCALEPACK |
| Phasing software | PHASER |
| Refinement software | PHENIX ((1.10.1_2155: ???)) |
Quality characteristics
| Overall | Inner shell | Outer shell | |
| 分解能 [Å] (低) | 50.000 | 50.000 | 2.540 |
| 分解能 [Å] (高) | 2.493 | 6.780 | 2.500 |
| Rmerge_l_obs | 0.102 | 0.055 | |
| Rmeas | 0.107 | 0.058 | |
| Rpim | 0.036 | 0.018 | 0.485 |
| 独立反射数 | 29938 | ||
| <I/σ(I)> | 12.6 | ||
| 完全性 [%] | 99.8 | 98.6 | 100 |
| 冗長性 | 10.9 | 10.7 | 10.6 |
| CC(1/2) | 0.997 | 0.798 |
結晶化条件
| 結晶ID | 方法 | pH | 温度 | 溶液条件 |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | PEG 3350, KCl |
