5XF7
Crystal structure of human protein disulfide isomerase-like protein of the testis
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-11-11 |
Detector | APEX II CCD |
Wavelength(s) | 0.987 |
Spacegroup name | P 32 |
Unit cell lengths | 97.361, 97.361, 57.588 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.420 |
High resolution limit [Å] | 2.380 | 2.380 |
Number of reflections | 24401 | |
<I/σ(I)> | 20.6 | 2 |
Completeness [%] | 99.8 | 100 |
Redundancy | 3.8 | 3.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 289 | 21% (w/v) PEG 3350 and 0.1 M succinic acid, pH 7.0 |