5XDZ
Crystal structure of zebrafish SNX25 PX domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-01-05 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.9785 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 68.150, 82.830, 36.500 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 52.627 - 1.700 |
R-factor | 0.1912 |
Rwork | 0.189 |
R-free | 0.23710 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4pqo |
RMSD bond length | 0.013 |
RMSD bond angle | 1.346 |
Data scaling software | Aimless (0.5.17) |
Phasing software | MOLREP |
Refinement software | PHENIX |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 68.150 | 68.150 | 1.730 |
High resolution limit [Å] | 1.700 | 9.000 | 1.700 |
Rmerge | 0.053 | 0.076 | 0.276 |
Rmeas | 0.057 | 0.082 | 0.298 |
Rpim | 0.020 | 0.028 | 0.108 |
Total number of observations | 155855 | 1207 | 8275 |
Number of reflections | 23068 | ||
<I/σ(I)> | 12.6 | 24.1 | 2.5 |
Completeness [%] | 98.7 | 96.9 | 99.2 |
Redundancy | 6.8 | 6.2 | 6.8 |
CC(1/2) | 0.998 | 0.991 | 0.969 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 6.5 | 293 | 1.6M Sodium citrate tribasic dihydrate pH 6.5 |