5WXU
11S globulin from Wrightia tinctoria reveals auxin binding site
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM14 |
Synchrotron site | ESRF |
Beamline | BM14 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-04-22 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 1 |
Spacegroup name | P 21 21 21 |
格子定数 [Å] | 111.209, 114.242, 202.479 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 101.240 - 1.700 |
R因子 | 0.17677 |
Rwork | 0.174 |
R-free | 0.22718 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3ehk |
結合長の平均二乗偏差(RMSD) [Å] | 0.020 |
結合角の平均二乗偏差(RMSD) [度] | 2.175 |
Data reduction software | MxCuBE |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0158) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 101.200 | 1.730 |
分解能 [Å] (高) | 1.700 | 1.700 |
独立反射数 | 270464 | |
<I/σ(I)> | 16.77 | 2.34 |
完全性 [%] | 94.2 | 92.43 |
冗長性 | 3.9 | 3.3 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 293 | 0.2 M Sodium citrate tribasic dihydrate, 100 mM Tris hydrochloride pH 8.5, 30% v/v PEG 400 |