5WXC

Crystal Structure of HLA-A*2402 in complex with avian influenza A(H7N9) virus-derived peptide H7-25 (data set 2)

Experimental procedure

実験手法	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U
Synchrotron site	SSRF
Beamline	BL17U
Temperature [K]	100
Detector technology	PIXEL
Collection date	2014-11-15
Detector	SDMS
Wavelength(s)	0.97930
Spacegroup name	P 1 21 1
格子定数 [Å]	81.373, 67.292, 88.346
格子定数 [度]	90.00, 98.43, 90.00

精密化法

残基	30.824 - 2.295
R因子	0.1791
Rwork	0.177
R-free	0.22400
結合長の平均二乗偏差(RMSD) [Å]	0.006
結合角の平均二乗偏差(RMSD) [度]	0.855
Data reduction software	CNS
Data scaling software	CNS
Phasing software	CNS
Refinement software	PHENIX ((1.10.1_2155))

Quality characteristics

	Overall
分解能 [Å] (低)	50.000
分解能 [Å] (高)	2.295
独立反射数	42274
<I/σ(I)>	18.155
完全性 [%]	99.1
冗長性	4.5

結晶化条件

結晶ID	方法	pH	温度	溶液条件
1	VAPOR DIFFUSION, HANGING DROP	6	291	0.1 M MES monohydrate pH 6.0, 14% w/v Polyethylene glycol 4000