5O5Q
X-ray crystal structure of RapZ from Escherichia coli (P3221 space group)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.1 |
Synchrotron site | BESSY |
Beamline | 14.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-05-01 |
Detector | RAYONIX MX-225 |
Wavelength(s) | 0.91841 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 91.540, 91.540, 352.550 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 45.770 - 3.250 |
R-factor | 0.2204 |
Rwork | 0.218 |
R-free | 0.27290 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.004 |
RMSD bond angle | 0.734 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((dev_2747: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.770 | 3.366 |
High resolution limit [Å] | 3.250 | 3.250 |
Rmerge | 0.086 | 0.762 |
Number of reflections | 27399 | |
<I/σ(I)> | 13.37 | 2.56 |
Completeness [%] | 97.6 | |
Redundancy | 4.67 | 4.77 |
CC(1/2) | 0.998 | 0.768 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 277 | 0.1 M MES,1 M ammonium sulfate, 0.01 M mercaptoethanol, 1%(v/v) glycerol pH 7.0 |