5FCD
Crystal structure of MccD protein
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-03-11 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9794 |
Spacegroup name | P 63 |
格子定数 [Å] | 95.100, 95.100, 128.685 |
格子定数 [度] | 90.00, 90.00, 120.00 |
精密化法
残基 | 39.220 - 2.100 |
R因子 | 0.2004 |
Rwork | 0.199 |
R-free | 0.22280 |
Structure solution method | SAD |
結合長の平均二乗偏差(RMSD) [Å] | 0.003 |
結合角の平均二乗偏差(RMSD) [度] | 0.702 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | HKL-3000 |
Refinement software | PHENIX (dev_1888) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 39.220 | 2.140 |
分解能 [Å] (高) | 2.100 | 2.100 |
Rmerge_l_obs | 0.049 | |
独立反射数 | 38222 | |
<I/σ(I)> | 19 | |
完全性 [%] | 99.3 | 99.9 |
冗長性 | 4.6 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 293 | 1.6 M Na Citrate |