4ZHS
Crystal Structure of Aspartate Semialdehyde Dehydrogenase from Trichophyton rubrum
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-04-19 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.979 |
Spacegroup name | P 31 2 1 |
格子定数 [Å] | 157.504, 157.504, 188.401 |
格子定数 [度] | 90.00, 90.00, 120.00 |
精密化法
残基 | 27.621 - 2.603 |
R因子 | 0.2158 |
Rwork | 0.214 |
R-free | 0.25680 |
結合長の平均二乗偏差(RMSD) [Å] | 0.007 |
結合角の平均二乗偏差(RMSD) [度] | 1.059 |
Refinement software | PHENIX (1.7.3_928) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 27.621 | 2.760 |
分解能 [Å] (高) | 2.600 | 2.600 |
Rmerge_l_obs | 0.096 | 0.693 |
独立反射数 | 311564 | |
<I/σ(I)> | 7.24 | 1.56 |
完全性 [%] | 97.2 | 97.1 |
冗長性 | 1.87 | 1.86 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 5.4 | 293 | 0.2M Ammonium Sulfate, 0.1M Sodium citrate pH5.4, 15% PEG 4000 |