4YYB
The structure of hemagglutinin from a H6N1 influenza virus (A/Taiwan/2/2013) in complex with human receptor analog 6'SLNLN
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-09-10 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9793 |
Spacegroup name | P 63 |
Unit cell lengths | 114.387, 114.387, 166.049 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 39.774 - 2.609 |
R-factor | 0.1941 |
Rwork | 0.192 |
R-free | 0.22650 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.111 |
Data reduction software | SCALA |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX (1.8.3_1479) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.690 |
High resolution limit [Å] | 2.609 | 2.600 |
Rmerge | 0.137 | 0.846 |
Number of reflections | 37317 | |
<I/σ(I)> | 21.2 | 3.8 |
Completeness [%] | 99.9 | 99.9 |
Redundancy | 12.2 | 12.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291.15 | 0.2M ammonium acetate, 0.1M sodium acetate pH4.0, 15%(w/v) PEG4000 |