4UV9
LSD1(KDM1A)-CoREST in complex with 1-Ethyl-Tranylcypromine
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Detector | DECTRIS PIXEL |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 118.300, 178.560, 234.020 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 53.230 - 3.000 |
R-factor | 0.22654 |
Rwork | 0.226 |
R-free | 0.24585 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2v1d |
RMSD bond length | 0.005 |
RMSD bond angle | 0.976 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0027) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 53.000 | 3.160 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.140 | 1.060 |
Number of reflections | 49581 | |
<I/σ(I)> | 7.5 | 1.3 |
Completeness [%] | 99.5 | 99.8 |
Redundancy | 3.4 | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | PH 6.5 |