4UN8
THE CRYSTAL STRUCTURE OF I-DMOI IN COMPLEX WITH ITS TARGET DNA AT 1H INCUBATION IN 5MM MN (STATE 2)
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 1 21 1 |
格子定数 [Å] | 107.186, 70.851, 107.232 |
格子定数 [度] | 90.00, 119.55, 90.00 |
精密化法
残基 | 46.642 - 2.600 |
R因子 | 0.1806 |
Rwork | 0.178 |
R-free | 0.22310 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2vs7 |
結合長の平均二乗偏差(RMSD) [Å] | 0.010 |
結合角の平均二乗偏差(RMSD) [度] | 1.212 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 46.640 | 2.740 |
分解能 [Å] (高) | 2.600 | 2.600 |
Rmerge_l_obs | 0.070 | 0.650 |
独立反射数 | 42078 | |
<I/σ(I)> | 15.4 | 2.4 |
完全性 [%] | 97.3 | 95.6 |
冗長性 | 4.8 | 4.9 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | 6 | pH 6 |