4O0P
Crystal Structure of D. radiodurans Bacteriophytochrome Photosensory Core Module in its Dark Form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-06-28 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.98044 |
Spacegroup name | P 64 |
Unit cell lengths | 150.280, 150.280, 145.950 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 48.650 - 3.800 |
R-factor | 0.2536 |
Rwork | 0.253 |
R-free | 0.26570 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2o9c |
RMSD bond length | 0.006 |
RMSD bond angle | 1.112 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 48.650 | 3.900 | |
High resolution limit [Å] | 3.800 | 15.000 | 3.800 |
Rmerge | 0.392 | 0.147 | 4.513 |
Rmeas | 0.156 | 4.725 | |
Number of reflections | 18551 | 310 | 1362 |
<I/σ(I)> | 4.72 | 12.48 | 1.05 |
Completeness [%] | 99.9 | 96.9 | 100 |
Redundancy | 10.97 | 9.6 | 11.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 298 | 30% PEG 1500, in dark, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 298.0K |