4JNT
Crystal structure of the ectodomain of Bovine viral diarrhea virus 1 E2 envelope protein
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 195 |
Detector technology | CCD |
Collection date | 2011-04-06 |
Detector | ADSC QUANTUM 315 |
Spacegroup name | C 1 2 1 |
格子定数 [Å] | 155.632, 67.885, 139.406 |
格子定数 [度] | 90.00, 121.89, 90.00 |
精密化法
残基 | 48.570 - 4.090 |
R因子 | 0.323 |
Rwork | 0.321 |
R-free | 0.37600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4ild |
結合長の平均二乗偏差(RMSD) [Å] | 0.012 |
結合角の平均二乗偏差(RMSD) [度] | 1.894 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0029) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 50.000 | 4.340 |
分解能 [Å] (高) | 4.090 | 4.090 |
Rmerge_l_obs | 1.002 | |
独立反射数 | 18935 | |
<I/σ(I)> | 4.78 | 1.34 |
完全性 [%] | 98.1 | 98.1 |
冗長性 | 2.12 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | 5.5 | 294 | 10% polyethylene glycol 3350, 0.1 M Bis-tris pH 5.5, 0.05 M cesium chloride, 0.04 M calcium acetate, 10% glycerol, VAPOR DIFFUSION, SITTING DROP, temperature 294K |