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4IPX

Analyzing the visible conformational substates of the FK506 binding protein FKBP12

Experimental procedure
実験手法SINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsCu FINE FOCUS
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date2012-10-28
DetectorRIGAKU RAXIS IV++
Wavelength(s)1.5418
Spacegroup nameC 1 2 1
格子定数 [Å]70.550, 35.948, 40.923
格子定数 [度]90.00, 95.89, 90.00
精密化法
残基19.607 - 1.700
R因子0.2072
Rwork0.207
R-free0.21750
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2ppn
結合長の平均二乗偏差(RMSD) [Å]0.006
結合角の平均二乗偏差(RMSD) [度]1.111
Data reduction softwareCrystalClear
Data scaling softwareCrystalClear
Phasing softwarePHENIX
Refinement softwarePHENIX ((phenix.refine: 1.7.3_928))
Quality characteristics
 OverallOuter shell
分解能 [Å] (低)35.0001.760
分解能 [Å] (高)1.7001.700
Rmerge_l_obs0.0970.296
独立反射数10996
<I/σ(I)>29.46.3
完全性 [%]93.793.6
冗長性3.233.4
結晶化条件
結晶ID方法pH温度溶液条件
1VAPOR DIFFUSION, HANGING DROP7.42981.7 M sodium malonate, pH 7.0, 0.1 M HEPES, pH 7.4, 5% MPD, VAPOR DIFFUSION, HANGING DROP, temperature 298K

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件を2024-09-18に公開中

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