4HFL
Crystal structure of the type VI effector Tae4 from Enterobacter cloacae
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BSRF BEAMLINE 3W1A |
Synchrotron site | BSRF |
Beamline | 3W1A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-06-20 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 0.9793 |
Spacegroup name | P 32 2 1 |
格子定数 [Å] | 84.283, 84.283, 43.452 |
格子定数 [度] | 90.00, 90.00, 120.00 |
精密化法
残基 | 23.290 - 2.002 |
R因子 | 0.2084 |
Rwork | 0.208 |
R-free | 0.25120 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4hff |
結合長の平均二乗偏差(RMSD) [Å] | 0.009 |
結合角の平均二乗偏差(RMSD) [度] | 1.136 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.7.3_928)) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 50.000 | 2.030 |
分解能 [Å] (高) | 2.000 | 2.000 |
Rmerge_l_obs | 0.070 | 0.142 |
独立反射数 | 12215 | |
<I/σ(I)> | 44.3 | 11.1 |
完全性 [%] | 100.0 | 98.5 |
冗長性 | 5.1 | 4.8 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, SITTING DROP | 5.6 | 293 | 0.5M Ammonium sulfate, 0.1M Sodium citrate tribasic dehydrate pH5.6, 1.0M Lithium sulfate monohydrate, VAPOR DIFFUSION, SITTING DROP, temperature 293K |