4ETX
Crystal Structure of PelD 158-CT from Pseudomonas aeruginosa PAO1
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-F |
Synchrotron site | APS |
Beamline | 21-ID-F |
Detector technology | IMAGE PLATE |
Detector | MAR scanner 300 mm plate |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 21 1 |
格子定数 [Å] | 60.290, 42.440, 60.470 |
格子定数 [度] | 90.00, 112.78, 90.00 |
精密化法
残基 | 25.000 - 2.000 |
R因子 | 0.2346 |
Rwork | 0.232 |
R-free | 0.28520 |
Structure solution method | SAD |
結合長の平均二乗偏差(RMSD) [Å] | 0.012 |
結合角の平均二乗偏差(RMSD) [度] | 1.351 |
Data scaling software | XSCALE |
Refinement software | REFMAC (5.5.0109) |
Quality characteristics
Overall | Inner shell | Outer shell | |
分解能 [Å] (低) | 2.100 | ||
分解能 [Å] (高) | 2.000 | 50.000 | 2.000 |
Rmerge_l_obs | 0.047 | 0.468 | |
独立反射数 | 19307 | 2590 | |
<I/σ(I)> | 24.69 | 4.04 | |
完全性 [%] | 99.8 | 99.7 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | hanging drop | 8 | 298 | 100 mM Tris, pH 8, 200 mM MgCl2, 10% (v/v) PEG 8000, hanging drop, temperature 298K |