Loading
PDBj
メニューPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

4EPW

Discovery of Small Molecules that Bind to K-Ras and Inhibit Sos-mediated Activation

Experimental procedure
実験手法SINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsBRUKER AXS MICROSTAR
Temperature [K]100
Detector technologyCCD
Collection date2010-04-01
DetectorBruker Platinum 135
Wavelength(s)1.5418
Spacegroup nameP 21 21 21
格子定数 [Å]39.219, 41.924, 91.448
格子定数 [度]90.00, 90.00, 90.00
精密化法
残基45.720 - 1.700
R因子0.1883
Rwork0.186
R-free0.24000
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)4epv
結合長の平均二乗偏差(RMSD) [Å]0.026
結合角の平均二乗偏差(RMSD) [度]2.078
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwareMOLREP
Refinement softwareREFMAC (5.6.0119)
Quality characteristics
 OverallOuter shell
分解能 [Å] (低)45.7201.730
分解能 [Å] (高)1.7001.700
Rmerge_l_obs0.1060.151
独立反射数16370
<I/σ(I)>8.64.3
完全性 [%]94.483.8
冗長性1.8
結晶化条件
結晶ID方法pH温度溶液条件
1VAPOR DIFFUSION, SITTING DROP29132% PEG1500, 0.7% 1-Butanol, pH 6.1-8.7, VAPOR DIFFUSION, SITTING DROP, temperature 291K

225158

件を2024-09-18に公開中

PDB statisticsPDBj update infoContact PDBjnumon