4CWQ

Human HSP90 alpha N-terminal domain in complex with an Aminotriazoloquinazoline inhibitor

Experimental procedure

実験手法	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU MICROMAX-007 HF
Temperature [K]	100
Detector technology	IMAGE PLATE
Collection date	2008-01-17
Detector	MAR scanner 345 mm plate
Spacegroup name	I 2 2 2
格子定数 [Å]	67.060, 91.007, 98.607
格子定数 [度]	90.00, 90.00, 90.00

精密化法

残基	30.000 - 2.000
R因子	0.19856
Rwork	0.196
R-free	0.24038
Structure solution method	OTHER
Starting model (for MR)	NONE
結合長の平均二乗偏差(RMSD) [Å]	0.011
結合角の平均二乗偏差(RMSD) [度]	1.321
Data reduction software	DENZO
Data scaling software	SCALEPACK
Refinement software	REFMAC (5.6.0117)

Quality characteristics

	Overall	Outer shell
分解能 [Å] (低)	30.000	2.070
分解能 [Å] (高)	2.000	2.000
Rmerge_l_obs	0.040	0.170
独立反射数	19797
<I/σ(I)>	17	5.8
完全性 [%]	94.8	94.6
冗長性	5.4

結晶化条件

結晶ID	方法	pH	温度	溶液条件
1