4CWQ
Human HSP90 alpha N-terminal domain in complex with an Aminotriazoloquinazoline inhibitor
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2008-01-17 |
Detector | MAR scanner 345 mm plate |
Spacegroup name | I 2 2 2 |
格子定数 [Å] | 67.060, 91.007, 98.607 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 30.000 - 2.000 |
R因子 | 0.19856 |
Rwork | 0.196 |
R-free | 0.24038 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
結合長の平均二乗偏差(RMSD) [Å] | 0.011 |
結合角の平均二乗偏差(RMSD) [度] | 1.321 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | REFMAC (5.6.0117) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 30.000 | 2.070 |
分解能 [Å] (高) | 2.000 | 2.000 |
Rmerge_l_obs | 0.040 | 0.170 |
独立反射数 | 19797 | |
<I/σ(I)> | 17 | 5.8 |
完全性 [%] | 94.8 | 94.6 |
冗長性 | 5.4 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 |