4BQJ

structure of HSP90 with an inhibitor bound

Experimental procedure

実験手法	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU MICROMAX-007 HF
Temperature [K]	100
Detector technology	IMAGE PLATE
Collection date	2008-04-07
Detector	MAR scanner 345 mm plate
Spacegroup name	P 1 21 1
格子定数 [Å]	53.699, 40.855, 54.221
格子定数 [度]	90.00, 115.83, 90.00

精密化法

残基	30.000 - 2.000
R因子	0.19224
Rwork	0.191
R-free	0.22089
Structure solution method	MOLECULAR REPLACEMENT
結合長の平均二乗偏差(RMSD) [Å]	0.008
結合角の平均二乗偏差(RMSD) [度]	1.229
Data reduction software	DENZO
Data scaling software	SCALEPACK
Refinement software	REFMAC (5.6.0117)

Quality characteristics

	Overall	Outer shell
分解能 [Å] (低)	30.000	2.070
分解能 [Å] (高)	2.000	2.000
Rmerge_l_obs	0.080	0.270
独立反射数	14089
<I/σ(I)>	12.6	4
完全性 [%]	97.1	82.1
冗長性	3.5

結晶化条件

結晶ID	方法	pH	温度	溶液条件
1