4BQG

structure of HSP90 with an inhibitor bound

Experimental procedure

実験手法	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU MICROMAX-007 HF
Temperature [K]	100
Detector technology	IMAGE PLATE
Collection date	2007-12-05
Detector	MAR scanner 345 mm plate
Spacegroup name	I 2 2 2
格子定数 [Å]	67.807, 90.346, 98.471
格子定数 [度]	90.00, 90.00, 90.00

精密化法

残基	66.520 - 1.900
R因子	0.20204
Rwork	0.200
R-free	0.23496
Structure solution method	MOLECULAR REPLACEMENT
結合長の平均二乗偏差(RMSD) [Å]	0.011
結合角の平均二乗偏差(RMSD) [度]	1.395
Data reduction software	DENZO
Data scaling software	SCALEPACK
Refinement software	REFMAC (5.6.0117)

Quality characteristics

	Overall	Outer shell
分解能 [Å] (低)	30.000	1.970
分解能 [Å] (高)	1.900	1.900
Rmerge_l_obs	0.060	0.550
独立反射数	23787
<I/σ(I)>	17	3.5
完全性 [%]	98.2	96.7
冗長性	5.5

結晶化条件

結晶ID	方法	pH	温度	溶液条件
1