4A14
HUMAN KIF7, A KINESIN INVOLVED IN HEDGEHOG SIGNALLING
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 93 |
Detector technology | PIXEL |
Collection date | 2010-07-19 |
Detector | DECTRIS PILATUS 2M |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 45.991, 79.799, 95.094 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.459 - 1.600 |
R-factor | 0.1837 |
Rwork | 0.182 |
R-free | 0.20670 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3b6v |
RMSD bond length | 0.011 |
RMSD bond angle | 1.547 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 1.690 |
High resolution limit [Å] | 1.500 | 1.600 |
Rmerge | 0.030 | 0.430 |
Number of reflections | 46998 | |
<I/σ(I)> | 30.1 | 4.4 |
Completeness [%] | 100.0 | 100 |
Redundancy | 7.5 | 7.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 20% POLYETHYLENE GLYCOL 3350, 0.20 M LITHIUM ACETATE. |