3WKL
The periplasmic PDZ tandem fragment of the RseP homologue from Aquifex aeolicus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-17A |
Synchrotron site | Photon Factory |
Beamline | BL-17A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-01-21 |
Detector | ADSC QUANTUM 270 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 78.861, 78.861, 211.822 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.100 | 2.950 |
High resolution limit [Å] | 2.800 | 2.800 |
Number of reflections | 10257 | |
Completeness [%] | 99.8 | 99.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4.5 | 1.5M AMMONIUM SULFATE, 0.1M SODIUM ACCETATE, PH 4.5, VAPOR DIFFUSION, HANGING DROP, TEMPERATURE 293K |