3WGE
Crystal structure of ERp46 Trx2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL44XU |
Synchrotron site | SPring-8 |
Beamline | BL44XU |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-07-03 |
Detector | RAYONIX MX225HE |
Wavelength(s) | 0.7 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 32.580, 39.060, 87.200 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 12.476 - 0.950 |
R-factor | 0.1228 |
Rwork | 0.122 |
R-free | 0.13480 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.012 |
RMSD bond angle | 1.370 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.8.2_1309)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 12.570 | 1.000 |
High resolution limit [Å] | 0.950 | 0.950 |
Number of reflections | 70957 | |
Completeness [%] | 99.9 | 100 |
Redundancy | 7.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.4 | 293 | 0.1M HEPES, 2.2M Ammonium sulfate, pH 7.4, VAPOR DIFFUSION, SITTING DROP, temperature 293K |