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3VYT

Crystal structure of the HypC-HypD-HypE complex (form I inward)

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSPRING-8 BEAMLINE BL41XU
Synchrotron siteSPring-8
BeamlineBL41XU
Temperature [K]100
Detector technologyCCD
Collection date2009-06-12
DetectorRAYONIX MX225HE
Wavelength(s)1.0000
Spacegroup nameC 1 2 1
Unit cell lengths78.333, 99.412, 103.923
Unit cell angles90.00, 97.79, 90.00
Refinement procedure
Resolution34.790 - 2.250
R-factor0.207
Rwork0.207
R-free0.25300
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2z1c 2z1d 2z1e
RMSD bond length0.011
RMSD bond angle1.500
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwareMOLREP
Refinement softwareCNS (1.2)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.300
High resolution limit [Å]2.2502.250
Number of reflections34520
<I/σ(I)>23.222.3
Completeness [%]92.180.4
Redundancy32
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP6.429350mM MES, 12-16% PEG400, 10mM magnesium chloride, pH 6.4, VAPOR DIFFUSION, SITTING DROP, temperature 293K

225158

数据于2024-09-18公开中

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