Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

3QFZ

Crystal Structure of Cellvibrio gilvus Cellobiose Phosphorylase Complexed with Sulfate and 1-Deoxynojirimycin

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsPHOTON FACTORY BEAMLINE AR-NW12A
Synchrotron sitePhoton Factory
BeamlineAR-NW12A
Temperature [K]100
Detector technologyCCD
Collection date2007-12-01
DetectorADSC QUANTUM 210
Wavelength(s)1.0
Spacegroup nameP 1 21 1
Unit cell lengths84.906, 98.128, 104.778
Unit cell angles90.00, 102.53, 90.00
Refinement procedure
Resolution36.270 - 2.390
R-factor0.14417
Rwork0.141
R-free0.20824
Structure solution methodFOURIER SYNTHESIS
RMSD bond length0.018
RMSD bond angle1.665
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Refinement softwareREFMAC (5.2.0019)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.490
High resolution limit [Å]2.3902.400
Number of reflections65851
<I/σ(I)>12.53.2
Completeness [%]99.799.6
Redundancy3.83.7
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP7.52981.6M ammonium sulfate, 0.1M HEPES-NaOH, 10mM glucose, 10mM 1-deoxynojirimycin, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 298.0K

225158

건을2024-09-18부터공개중

PDB statisticsPDBj update infoContact PDBjnumon