Loading
PDBj
メニューPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

3NSW

Crystal Structure of Ancylostoma ceylanicum Excretory-Secretory Protein 2

Experimental procedure
実験手法SINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsNSLS BEAMLINE X25
Synchrotron siteNSLS
BeamlineX25
Temperature [K]100
Detector technologyCCD
Collection date2009-07-28
DetectorADSC QUANTUM 315
Wavelength(s)1.0809
Spacegroup nameP 43
格子定数 [Å]52.212, 52.212, 345.263
格子定数 [度]90.00, 90.00, 90.00
精密化法
残基36.910 - 1.750
R因子0.14773
Rwork0.146
R-free0.17466
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)STARTING MODEL: THE STRUCTURE OF ACEES-2 WAS SOLVED USING A LEAD (PBNO3) SOAKED CRYSTAL AND SAD METHODS AT 2.0 ANGSTROM RESOLUTION
結合長の平均二乗偏差(RMSD) [Å]0.009
結合角の平均二乗偏差(RMSD) [度]1.122
Data reduction softwareHKL-2000
Data scaling softwareSCALEPACK
Phasing softwarePHASER
Refinement softwareREFMAC (5.5.0109)
Quality characteristics
 OverallOuter shell
分解能 [Å] (低)36.9101.810
分解能 [Å] (高)1.7501.750
Rmerge_l_obs0.0740.354
独立反射数79362
<I/σ(I)>18.4982.326
完全性 [%]90.552.3
冗長性4.61.9
結晶化条件
結晶ID方法pH温度溶液条件
1VAPOR DIFFUSION, HANGING DROP6.82770.1 M 2-[4-(2-hydroxyethyl)piperazin-1-yl]ethanesulfonic acid (HEPES), 60% (4S)-2-Methyl-2,4-pentanediol (MPD), pH 6.8, VAPOR DIFFUSION, HANGING DROP, temperature 277K

225158

件を2024-09-18に公開中

PDB statisticsPDBj update infoContact PDBjnumon