3FBB
Crystal structure of the Mimivirus NDK N62L-R107G double mutant complexed with UDP
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-1 |
Synchrotron site | ESRF |
Beamline | ID14-1 |
Temperature [K] | 105 |
Detector technology | CCD |
Collection date | 2007-09-09 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 0.934 |
Spacegroup name | C 2 2 21 |
格子定数 [Å] | 79.676, 152.899, 184.534 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 28.549 - 2.400 |
R因子 | 0.184 |
Rwork | 0.181 |
R-free | 0.22700 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2b8p |
結合長の平均二乗偏差(RMSD) [Å] | 0.009 |
結合角の平均二乗偏差(RMSD) [度] | 1.272 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | AMoRE |
Refinement software | PHENIX ((phenix.refine)) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 70.000 | 2.530 |
分解能 [Å] (高) | 2.400 | 2.400 |
独立反射数 | 44282 | |
<I/σ(I)> | 10.5 | 2.3 |
完全性 [%] | 99.6 | 99.8 |
冗長性 | 6.7 | 6.8 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 7.4 | 293 | 40-44% MPD, 0.1M MOPS, pH 7.4, VAPOR DIFFUSION, HANGING DROP, temperature 293K |