3EWQ
HCov-229E Nsp3 ADRP domain
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-5A |
Synchrotron site | Photon Factory |
Beamline | BL-5A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-02-03 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9798 |
Spacegroup name | P 21 21 21 |
格子定数 [Å] | 47.820, 50.852, 68.278 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 30.000 - 2.100 |
R因子 | 0.20842 |
Rwork | 0.204 |
R-free | 0.28233 |
Structure solution method | SAD |
結合長の平均二乗偏差(RMSD) [Å] | 0.019 |
結合角の平均二乗偏差(RMSD) [度] | 1.886 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SOLVE |
Refinement software | REFMAC (5.2.0019) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 50.000 | 2.150 |
分解能 [Å] (高) | 2.100 | 2.100 |
Rmerge_l_obs | 0.234 | 0.234 |
独立反射数 | 9732 | |
<I/σ(I)> | 6.2 | |
完全性 [%] | 96.4 | 99.6 |
冗長性 | 12 | 12 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION | 7.5 | 291 | 0.1M HEPES pH 7.5, 25% w/v PEG 3350, VAPOR DIFFUSION, temperature 291.0K |