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3ED9

Carbonmonoxy Sperm Whale Myoglobin at 140 K: Laser on [30 min]

Experimental procedure
実験手法SINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsPHOTON FACTORY BEAMLINE AR-NW14A
Synchrotron sitePhoton Factory
BeamlineAR-NW14A
Temperature [K]140
Detector technologyCCD
Collection date2008-02-20
DetectorMAR CCD 165 mm
Wavelength(s)0.827
Spacegroup nameP 1 21 1
格子定数 [Å]34.347, 30.620, 63.799
格子定数 [度]90.00, 105.87, 90.00
精密化法
残基16.750 - 1.210
R因子0.17
Rwork0.167
R-free0.22000
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1mbc
結合長の平均二乗偏差(RMSD) [Å]0.035
結合角の平均二乗偏差(RMSD) [度]2.971
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareMOLREP
Refinement softwareREFMAC
Quality characteristics
 OverallInner shellOuter shell
分解能 [Å] (低)50.00050.0001.250
分解能 [Å] (高)1.2102.6101.210
Rmerge_l_obs0.0530.0230.533
独立反射数35228
<I/σ(I)>8.6
完全性 [%]88.998.235
冗長性3.43.61.6
結晶化条件
結晶ID方法pH温度溶液条件
1batch62932.4M Ammonium sulfate, 10mM TrisHCl, 100mM Sodium phosphate, pH 6.0, batch, temperature 293K

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件を2024-09-18に公開中

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