3ED9
Carbonmonoxy Sperm Whale Myoglobin at 140 K: Laser on [30 min]
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE AR-NW14A |
Synchrotron site | Photon Factory |
Beamline | AR-NW14A |
Temperature [K] | 140 |
Detector technology | CCD |
Collection date | 2008-02-20 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 0.827 |
Spacegroup name | P 1 21 1 |
格子定数 [Å] | 34.347, 30.620, 63.799 |
格子定数 [度] | 90.00, 105.87, 90.00 |
精密化法
残基 | 16.750 - 1.210 |
R因子 | 0.17 |
Rwork | 0.167 |
R-free | 0.22000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1mbc |
結合長の平均二乗偏差(RMSD) [Å] | 0.035 |
結合角の平均二乗偏差(RMSD) [度] | 2.971 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | REFMAC |
Quality characteristics
Overall | Inner shell | Outer shell | |
分解能 [Å] (低) | 50.000 | 50.000 | 1.250 |
分解能 [Å] (高) | 1.210 | 2.610 | 1.210 |
Rmerge_l_obs | 0.053 | 0.023 | 0.533 |
独立反射数 | 35228 | ||
<I/σ(I)> | 8.6 | ||
完全性 [%] | 88.9 | 98.2 | 35 |
冗長性 | 3.4 | 3.6 | 1.6 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | batch | 6 | 293 | 2.4M Ammonium sulfate, 10mM TrisHCl, 100mM Sodium phosphate, pH 6.0, batch, temperature 293K |