3BQJ

VA387 polypeptide

Experimental procedure

実験手法	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Temperature [K]	100
Detector technology	IMAGE PLATE
Collection date	2007-05-11
Detector	RIGAKU RAXIS IV++
Wavelength(s)	1.502
Spacegroup name	C 2 2 21
格子定数 [Å]	54.360, 96.800, 118.732
格子定数 [度]	90.00, 90.00, 90.00

精密化法

残基	99.000 - 2.700
Rwork	0.227
R-free	0.26700
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	CNS
Refinement software	CNS

Quality characteristics

	Overall	Inner shell	Outer shell
分解能 [Å] (低)	99.000	99.000	2.380
分解能 [Å] (高)	2.300	4.960	2.300
Rmerge_l_obs	0.071	0.032	0.234
独立反射数	11228
<I/σ(I)>	12.1
完全性 [%]	97.3	91.6	87.9
冗長性	3.5	3.8	3.1

結晶化条件

結晶ID	方法	pH	温度	溶液条件
1	VAPOR DIFFUSION, HANGING DROP	8.5	298	22% peg 4k, 3% 5-diaminopentane, tris, pH 8.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K