2X79
Inward facing conformation of Mhp1
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-06-13 |
Detector | ADSC QUANTUM 315 |
Spacegroup name | P 61 |
格子定数 [Å] | 173.888, 173.888, 74.502 |
格子定数 [度] | 90.00, 90.00, 120.00 |
精密化法
残基 | 33.388 - 3.800 |
R因子 | 0.2773 |
Rwork | 0.273 |
R-free | 0.31260 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
結合長の平均二乗偏差(RMSD) [Å] | 0.115 |
結合角の平均二乗偏差(RMSD) [度] | 1.037 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SHARP |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 40.000 | 3.940 |
分解能 [Å] (高) | 3.800 | 3.800 |
Rmerge_l_obs | 0.080 | 0.690 |
独立反射数 | 47973 | |
<I/σ(I)> | 17.6 | 1.4 |
完全性 [%] | 97.0 | 96 |
冗長性 | 3.8 | 2.8 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | 9 | 24-28% PEG300, 100 MM NACL AND 100 MM BICINE PH9.0 |