Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

2WLF

Crystallographic analysis of the polysialic acid O-acetyltransferase OatWY

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsALS BEAMLINE 4.2.2
Synchrotron siteALS
Beamline4.2.2
Temperature [K]100
Detector technologyCCD
Collection date2008-06-26
DetectorMBC NOIR-1
Spacegroup nameP 2 2 2
Unit cell lengths78.855, 94.656, 100.829
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution40.000 - 2.350
R-factor0.18504
Rwork0.183
R-free0.23094
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)IN-HOUSE STRUCTURE
RMSD bond length0.009
RMSD bond angle1.468
Data reduction softwareMOSFLM
Data scaling softwareSCALA
Phasing softwarePHASER
Refinement softwareREFMAC (5.5.0066)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]40.0002.480
High resolution limit [Å]2.3502.350
Rmerge0.1000.440
Number of reflections32150
<I/σ(I)>153.2
Completeness [%]100.0100
Redundancy4.84.9
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
14.6100 MM SODIUM ACETATE, 2.25 M AMMONIUM ACETATE, pH 4.6

225158

数据于2024-09-18公开中

PDB statisticsPDBj update infoContact PDBjnumon