2WAR
Hen Egg White Lysozyme E35Q chitopentaose complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Detector | RIGAKU IMAGE PLATE |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 78.632, 78.632, 36.700 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 14.760 - 1.800 |
R-factor | 0.157 |
Rwork | 0.155 |
R-free | 0.19600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1h6m |
RMSD bond length | 0.011 |
RMSD bond angle | 1.453 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | REFMAC (5.5.0082) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 15.000 | 1.860 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.050 | 0.280 |
Number of reflections | 11116 | |
<I/σ(I)> | 40 | 6.4 |
Completeness [%] | 93.0 | 95 |
Redundancy | 7 | 6.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4.5 | PROTEIN AT 7MG ML-1 IN 10MM CHITOPENTAOSE 200MM NA ACETATE PH5 WAS MIXED WITH RESERVOIR OF 200MM NA ACETATE, 4% W/V NACL PH4.5 |