2W6I
Low resolution structures of bovine mitochondrial F1-ATPase during controlled dehydration: Hydration State 4B.
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-2 |
Synchrotron site | ESRF |
Beamline | ID14-2 |
Temperature [K] | 294 |
Detector technology | CCD |
Collection date | 2008-10-30 |
Detector | ADSC CCD |
Spacegroup name | P 21 21 21 |
格子定数 [Å] | 108.920, 131.330, 267.380 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 30.000 - 4.000 |
R因子 | 0.299 |
Rwork | 0.299 |
R-free | 0.30000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1bmf |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0038) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 101.000 | 4.220 |
分解能 [Å] (高) | 4.000 | 4.000 |
Rmerge_l_obs | 0.220 | 0.600 |
独立反射数 | 30825 | |
<I/σ(I)> | 14.3 | 1.7 |
完全性 [%] | 93.3 | 94.5 |
冗長性 | 2.5 | 2.4 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | 8.5 | 50 MM TRIS-HCL PH 8.2, 200 MM NACL, 20 MM MGSO4, 1 MM ADP, 1 MM ALCL3, 6 MM NAF 0.004% (W/V)PHENYLMETHYLSULFONYL FLUORIDE AND 12% (W/V) POLYETHYLENE GLYCOL 6000 |