2VS8
The crystal structure of I-DmoI in complex with DNA and Mn
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 107.134, 70.634, 106.955 |
Unit cell angles | 90.00, 119.85, 90.00 |
Refinement procedure
Resolution | 25.760 - 2.100 |
R-factor | 0.203 |
Rwork | 0.201 |
R-free | 0.24800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2vs7 |
RMSD bond length | 0.012 |
RMSD bond angle | 1.698 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 26.820 | 2.210 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.050 | 0.450 |
Number of reflections | 80887 | |
<I/σ(I)> | 12.8 | 2.3 |
Completeness [%] | 99.7 | 99.5 |
Redundancy | 3 | 2.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.6% PEG 4000, 0.07M SODIUM ACETATE, PH 4.6-5.5, 30% GLYCEROL. |