2QRZ
Cdc42 bound to GMP-PCP: Induced Fit by Effector is Required
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CHESS BEAMLINE A1 |
Synchrotron site | CHESS |
Beamline | A1 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 0.978 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 98.500, 98.500, 102.400 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 31.270 - 2.400 |
Rwork | 0.234 |
R-free | 0.26300 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.400 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | CNS (1.2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 31.270 | |
High resolution limit [Å] | 2.400 | 2.400 |
Rmerge | 0.068 | |
Total number of observations | 2959 | |
Number of reflections | 20185 | |
<I/σ(I)> | 6.8 | |
Completeness [%] | 99.5 | |
Redundancy | 4.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 277 | 12% PEG 6K, 100 mM Na Acetate, 50 mM MES, pH 6.0, 100 mM Ammonium Sulfate, VAPOR DIFFUSION, HANGING DROP, temperature 277K |