2PXX
Human putative methyltransferase MGC2408
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-D |
Synchrotron site | APS |
Beamline | 23-ID-D |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-04-16 |
Detector | MARMOSAIC 300 mm CCD |
Wavelength(s) | 0.97926 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 35.883, 45.560, 55.102 |
Unit cell angles | 90.00, 105.87, 90.00 |
Refinement procedure
Resolution | 30.000 - 1.300 |
Rwork | 0.210 |
R-free | 0.22600 |
Structure solution method | SAD |
RMSD bond length | 0.016 |
RMSD bond angle | 1.317 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SHELX |
Refinement software | REFMAC (refmac_5.2.0019) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 70.000 | 70.000 | 1.350 |
High resolution limit [Å] | 1.300 | 2.800 | 1.300 |
Rmerge | 0.096 | 0.068 | 0.280 |
Number of reflections | 40375 | ||
<I/σ(I)> | 8.2 | ||
Completeness [%] | 96.2 | 99.7 | 74.1 |
Redundancy | 6.2 | 6.9 | 3.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 5.5 | 291 | 28% PEG3350, 0.1 M Ammonium sulfate, 0.1 M Bis-Tris, pH 5.5, VAPOR DIFFUSION, temperature 291K |
1 | VAPOR DIFFUSION | 5.5 | 291 | 28% PEG3350, 0.1 M Ammonium sulfate, 0.1 M Bis-Tris, pH 5.5, VAPOR DIFFUSION, temperature 291K |