2POO

THERMOSTABLE PHYTASE IN FULLY CALCIUM LOADED STATE

Experimental procedure

実験手法	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	MACSCIENCE M18X
Temperature [K]	297
Detector technology	IMAGE PLATE
Detector	MAC Science DIP-2020
Spacegroup name	P 21 21 21
格子定数 [Å]	50.980, 65.150, 105.680
格子定数 [度]	90.00, 90.00, 90.00

精密化法

残基	8.000 - 2.050
Rwork	0.228
R-free	0.26200
Structure solution method	MOLECULAR REPLACEMENT
結合長の平均二乗偏差(RMSD) [Å]	0.008
結合角の平均二乗偏差(RMSD) [度]	1.500
Data reduction software	DENZO
Data scaling software	SCALEPACK
Refinement software	X-PLOR (3.8)

Quality characteristics

	Overall
分解能 [Å] (低)	20.000
分解能 [Å] (高)	2.050
Rmerge_l_obs	0.060
独立反射数	21468
完全性 [%]	92.9
冗長性	2.5

結晶化条件

結晶ID	方法	pH	温度	溶液条件
1	other *	6.5		This particular structure is not described in this paper. *