2HX3

Rat nNOS heme domain complexed with (4S)-N-{4-Amino-5-[(2-aminoethyl)-hydroxyamino]-pentyl}-N'-nitroguanidine

Refinement Statistics

Experimental method:X-RAY DIFFRACTION (2 Å)

Cell axes51.910111.660164.210
Cell angles90.0090.0090.00
SpacegroupP 21 21 21
Resolution limits49.50 - 2.00
the highest resolution shell value2.130 - 2.000
R-factor0.217
R-work0.21700
the highest resolution shell value0.296
R-free0.25800
the highest resolution shell value0.325
RMSD bond length0.009
RMSD bond angle1.400

Data Collection Statistics

Resolution limits50.00 - 2.00
the highest resolution shell value -
Number of reflections65600
Rmerge_l_obs0.058
the highest resolution shell value0.559
Completeness99.7
Redundancy4.5
the highest resolution shell value4.5
I/sigma(I)-3

Crystallization Conditions

crystal IDmethodpHpH rangetemperatureunit
16280

Crystallization Reagents

IDcrystal IDsolution IDreagent nameconcentrationdetails
Crystallization Reagents in Literatures*
IDcrystal IDsolutionreagent nameconcentration (unit)details
Annotated Information is extracted from Literature Info*