2HRY
T. maritima PurL complexed with AMPPCP
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-02-10 |
Detector | MARMOSAIC 300 mm CCD |
Wavelength(s) | 0.9795 |
Spacegroup name | P 21 21 21 |
格子定数 [Å] | 56.617, 69.997, 133.476 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 19.880 - 2.800 |
R因子 | 0.185 |
Rwork | 0.185 |
R-free | 0.28300 |
Structure solution method | MOLECULAR REPLACEMENT |
結合長の平均二乗偏差(RMSD) [Å] | 0.010 |
結合角の平均二乗偏差(RMSD) [度] | 1.500 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | CNS |
Refinement software | CNS |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 19.880 | 2.980 |
分解能 [Å] (高) | 2.800 | 2.800 |
独立反射数 | 12807 | |
完全性 [%] | 94.3 | 88.9 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 7.1 | 298 | 17% PEG 4000, 8% Isopropanol, 0.1M HEPES, pH 7.1, VAPOR DIFFUSION, HANGING DROP, temperature 298K |