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2HHL

Crystal structure of the human small CTD phosphatase 3 isoform 1

Experimental procedure
実験手法SINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsNSLS BEAMLINE X6A
Synchrotron siteNSLS
BeamlineX6A
Temperature [K]100
Detector technologyCCD
Collection date2006-06-21
DetectorADSC QUANTUM 4
Wavelength(s)1.74
Spacegroup nameP 1 21 1
格子定数 [Å]47.419, 49.857, 179.747
格子定数 [度]90.00, 96.90, 90.00
精密化法
残基19.860 - 2.100
R因子0.191
Rwork0.188
R-free0.25200
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1ta0
結合長の平均二乗偏差(RMSD) [Å]0.022
結合角の平均二乗偏差(RMSD) [度]3.199
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareMOLREP
Refinement softwareREFMAC (5.2.0005)
Quality characteristics
 OverallOuter shell
分解能 [Å] (低)20.0002.180
分解能 [Å] (高)2.1002.100
Rmerge_l_obs0.0560.265
独立反射数47666
<I/σ(I)>8.5
完全性 [%]87.774
冗長性1.71.4
結晶化条件
結晶ID方法pH温度溶液条件
1VAPOR DIFFUSION, SITTING DROP5.52950.2M lithium sulfate monohydrate, 0.1M bis-tris, 25% w/v PEG 3350, pH 5.5, VAPOR DIFFUSION, SITTING DROP, temperature 295K

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件を2024-09-18に公開中

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