2FZU
Reduced enolate chromophore intermediate for GFP variant
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL7-1 |
Synchrotron site | SSRL |
Beamline | BL7-1 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2000-04-28 |
Detector | MARRESEARCH |
Wavelength(s) | 1.08 |
Spacegroup name | P 21 21 21 |
格子定数 [Å] | 51.350, 62.520, 71.750 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 20.000 - 1.250 |
Rwork | 0.142 |
R-free | 0.19900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ema |
結合長の平均二乗偏差(RMSD) [Å] | 0.022 |
結合角の平均二乗偏差(RMSD) [度] | 0.032 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | SHELXL-97 |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 20.000 | 1.290 |
分解能 [Å] (高) | 1.250 | 1.250 |
独立反射数 | 62613 | |
<I/σ(I)> | 19.6 | 2.3 |
完全性 [%] | 96.9 | 91.5 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 298 | 50 mM MgCl2, 50 mM Hepes, 20% PEG 4K, pH 8.0, VAPOR DIFFUSION, HANGING DROP, temperature 298K |