1ZNI
INSULIN
Experimental procedure
| Spacegroup name | H 3 |
| 格子定数 [Å] | 80.700, 80.700, 37.600 |
| 格子定数 [度] | 90.00, 90.00, 120.00 |
精密化法
| 残基 | 40.000 - 1.498 |
| Rwork | 0.178 |
| 結合長の平均二乗偏差(RMSD) [Å] | 0.023 |
| 結合角の平均二乗偏差(RMSD) [度] | 0.042 |
| Refinement software | REFMAC |
結晶化条件
| 結晶ID | 方法 | pH | 温度 | 溶液条件 |
| 1 | Batch method * | 5 * | Harding, M.M., (1966) J. Mol. Biol., 16, 212. * |
文献の結晶化試薬
| ID | 結晶ID | 溶液 | 試薬名 | 濃度 (単位) (単位) | 詳細 |
| 1 | 1 | 1 | insulin | 0.1g | |
| 2 | 1 | 1 | hydrochloric acid | 0.04 (M) | |
| 3 | 1 | 1 | zinc sulphate | 0.072 (M) | |
| 4 | 1 | 1 | trisodium citrate | 0.2 (M) | |
| 5 | 1 | 1 | 0.6g | ||
| 6 | 1 | 1 | 0.75 (M) | ||
| 7 | 1 | 1 | hydrochloric acid | 0.1 (M) |
